2026-06-08T12:21:09Z https://api.figshare.com/v2/oai

oai:figshare.com:article/23054465 2023-12-08T11:29:35Z category_25114 portal_549 item_type_3 month_year_12_2023

10.5522/04/23054465.v1 https://figshare.com/articles/dataset/XAFS_data_at_Pd_In_K-edges_recorded_in_situ_during_reduction_and_ex_situ_/23054465 https://ndownloader.figshare.com/files/40789724 https://ndownloader.figshare.com/files/40789727 https://ndownloader.figshare.com/files/40789730 https://ndownloader.figshare.com/files/40789733 https://ndownloader.figshare.com/files/40789736 https://ndownloader.figshare.com/files/40789739 Beale, Andrew Andrew Beale Allen, Lisa Lisa Allen Negahdar, Leila Leila Negahdar Inorganic green chemistry XAFS Catalyst Pd-In catalyst Al2O3 2023-12-08 2023-12-08 Dataset 2023 University College London X-ray absorption spectroscopy was performed at Diamond Light Source, UK, at B18 for the Pd/In2O3 & Pd/In2O3/Al2O3 species. Data was collected at the Pd and In K-edges in transmission mode using a QEXAFS setup with fast scanning Si(311) crystal monochromators. The time resolution here was roughly 90 seconds per spectrum. Samples were packed into an in-house custom-made capillary system designed and constructed by Diamond Light Source. 50 mg of 200-300 μm catalyst particles were packed between 3 cm of quartz wool.

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